High-temperature furnace for the CVT sample synthesis
- Two zones
- Thermocouple: K-type
- Maximal temperature: 1200°C
- Rated power: 3 kW
Vacuum sealing machine Partulab MRVS03A600
- Rotating speed: 0 – 30 rpm
- Quartz pipe outer diameter: 13 mm, 15 mm, 20 mm, 45 mm
- Tube wall thickness: ≤ 2 mm
- Vacuum level: 0.1 MPa – 10-5 Pa
Desktop X-ray Diffractometer Bruker D2 phaser
- X-ray line Cu Kα (1.54178 Å)
- Goniometer: θ – 2θ
- Angular accuracy: better than 0.02°
- Detector: SSD160-2, LYNXEYE-2
Scanning Electron Microscope HITACHI FlexSEM 1000 II
- Acceleration voltage: 0.3 kV – 20 kV
- Resolution: 4 nm (@ 20kV, high vacuum mode), 15 nm (@ 1kV, high vacuum mode)
- Vacuum level: 6 – 100 Pa
- Electron gun: Pre-centered cartridge filament
- Sample stage: motorized, x: 50 mm, y: 40 mm, z: 15 mm, tilt: -15 – 90°, azimuth: 360°
- Maximum sample size: diameter ≤ 80 mm, height ≤ 40 mm
Scanning Electron Microscope ZEISS Sigma500
- Acceleration voltage: 0.3 kV – 20 kV
- Image scanning resolution: 0.8 nm (@ 15kV), 1.6 nm (@ 1kV)
- Sample current range: 40 pA – 20 nA
- Magnification: 10x – 1000000x
- Electron emission source: Schottky field emission (thermal field emission)
- Detector: anngular secondary electron detector in mirror, secondary electron detector in sample chamber, backscattering electron detector, infrared CCD camera in sample chamber
Raman / Photoluminescent / Transient Life Spectrometer Nanofinder 30A
- Excitation light sources: lasers (442 nm, 532 nm, 785 nm), Picosec pulse diode laser (635 nm), one coherent femtosecond laser (400 – 900 nm)
- Raman shift range: 50 – 4000 cm-1
- Detectors: Cooled CCD detector (400 – 900 nm), Cooled InGaAs Detector (900 – 1400 nm), APD (350 – 900 nm), NIR-PMT/TSCPC(900 – 1700 nm)
- Temperature range: 5 K – 300 K
Glove Box MIKROUNA UNIVERSAL
- Controller: Siemens PLC
- Water content: < 0.1 ppm, Oxygen content: < 0.1 ppm
- Vacuum pump brand: Edwards, Extreme vacuum: 2×10-3 mbar
- Water analyzer brand: Xentaur, Range: 0.01 – 23000 ppm
- Oxygen anayzer brand: GE, Range can be set to 0 – 10, 100, 1000, 10000, 250000 ppm
UV-VIS, NIR Spectrometer PERKIN-ELMER, Lambda
- Wavelength coverage:190 – 3300 nm
- Wavelength accuracy: UV-Vis < 0.02 nm, NIR < 0.08 nm